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壳聚糖胍盐酸盐的制备及其在羊毛织物抗菌整理中的应用     被引量:3

Preparation of chitosan guanidine hydrochloride and application thereof in antimicrobial finishing of wool fabric

文献类型:期刊文献

中文题名:壳聚糖胍盐酸盐的制备及其在羊毛织物抗菌整理中的应用

英文题名:Preparation of chitosan guanidine hydrochloride and application thereof in antimicrobial finishing of wool fabric

作者:赵雪[1,2]

机构:[1]绍兴文理学院纺织服装学院;[2]浙江省清洁染整技术研究重点实验室

年份:2015

卷号:36

期号:4

起止页码:92

中文期刊名:纺织学报

外文期刊名:Journal of Textile Research

收录:CSTPCD、、北大核心2014、CSCD2015_2016、Scopus、北大核心、CSCD

基金:绍兴市科技计划公益技术应用研究项目(2014B70013)

语种:中文

中文关键词:壳聚糖胍盐酸盐;羊毛;抗菌整理;微波辐射

外文关键词:chitosan guanidine hydrochloride; wool; antimicrobial finishing; microwave irradiation

中文摘要:采用微波辐射技术,以壳聚糖胍亚硫酸盐和浓盐酸为原料,合成了一种壳聚糖胍盐酸盐抗菌剂,通过红外光谱和核磁谱图对其结构进行表征。将壳聚糖胍盐酸盐用于羊毛织物的抗菌整理,通过研究整理剂质量浓度、焙烘温度、焙烘时间对整理后羊毛织物抗菌效果和物理力学性能的影响优化整理工艺。结果表明,在微波辐射条件下成功合成了壳聚糖胍盐酸盐抗菌剂,整理剂在羊毛织物上的较佳整理工艺为壳聚糖胍盐质量浓度10 g/L,焙烘温度130℃,焙烘时间5 min。

外文摘要:Antimicrobial chitosan guanidine hydrochloride was synthesized by reacting chitosan guanidine sulfite with concentrated hydrochloric under microwave irradiation. The structures of guanidinylated chitosan were characterized by FT-IR and13 CNMR. Chitosan guanidine hydrochloride was applied to the antimicrobial finishing of wool fabric and the influences of finishing conditions including antimicrobial agent mass concentration,curing temperature and curing time on the antimicrobial effect and physical mechanical properties were researched. The results show that antimicrobial chitosan guanidine hydrochloride was synthesized successfully under microwave irradiation. The optimal process parameters for finishing agent on wool fabric are as followed: mass concentration of chitosan guanidine hydrochloride of 10 g / L,curing temperature of 130 ℃ and curing time of 5 min.

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