文献类型：期刊文献

英文题名：One-pot synthesis of beta-ketosulfones from sulfonyl chloride, hydrazine hydrate and vinyl azide in water

作者：Zhang, Yaohong[1];Luo, Mengqiang[1];Li, Yan[1];Shen, Runfu[1];Qi, Chenze[1];Wang, Hai[2];Cheng, Kai[1]

机构：[1]Shaoxing Univ, Sch Chem & Chem Engn, Zhejiang Key Lab Alternat Technol Fine Chem Proc, Shaoxing 312000, Zhejiang, Peoples R China;[2]Shaoxing Univ, Sch Life Sci, Shaoxing 312000, Zhejiang, Peoples R China

年份：2020

卷号：76

期号：48

外文期刊名：TETRAHEDRON

收录：SCI-EXPANDED(收录号：WOS:000590764800004)、、Scopus(收录号：2-s2.0-85093118576)、WOS、CCR-EXPANDED(收录号：WOS:000590764800004)

基金：We gratefully acknowledge the financial support from Zhejiang Provincial Natural Science foundation of China (No. LQ16H090004) and the National Natural Science Foundation of China (No. 31800292). We also thanks Anna Kerkula for English language editing.

语种：英文

外文关键词：One-pot synthesis; beta-Ketosulfones; Vinyl azides; Sulfonyl chloride; Hydrazine hydrate

外文摘要：A novel, facile and efficient strategy for the one-pot synthesis of beta-ketosulfones from readily available sulfonyl chloride, hydrazine hydrate and vinyl azides is described. The reaction proceeded very smoothly affording diverse beta-ketosulfones in moderate to good yields. This new procedure has the advantages of environmental benign, easy and simple operation, low cost and wide tolerance of functional groups, which provides a highly fascinating protocol to access beta-ketosulfones. (C) 2020 Elsevier Ltd. All rights reserved.