文献类型：期刊文献

英文题名：Determining Eight Biogenic Amines in Surface Water Using High-Performance Liquid Chromatography-Tandem Mass Spectrometry

作者：Quan, Zhengtao[1];Xie, Guangfa[2];Peng, Qi[1];Shan, Jicheng[1];Xing, Wenhao[1];Zhang, Jialei[1];Li, Shiling[1];Chan, Zhongyu[1];Chou, Chuanfeng[1];Zou, HuiJun[2]

机构：[1]Shaoxing Univ, Sch Life Sci, Shaoxing 312000, Peoples R China;[2]China Shaoxing Rice Wine Grp Co Ltd, Natl Engn Res Ctr Chinese Rice Wine, Shaoxing 312000, Peoples R China

年份：2016

卷号：25

期号：4

起止页码：1669

外文期刊名：POLISH JOURNAL OF ENVIRONMENTAL STUDIES

收录：SCI-EXPANDED(收录号：WOS:000381108800032)、、Scopus(收录号：2-s2.0-84992709242)、WOS

基金：We thank financial support provided by Shaoxing University Foundation (No. 20145031) and Xinmiao Talents Program in Zhejiang province (No. 2016R428024).

语种：英文

外文关键词：HPLC-MS/MS; surface water; biogenic amines

外文摘要：A method for determining eight biogenic amines in surface water was established using high-performance liquid chromatography-triple quadrupole mass spectrometry to improve on the detection sensitivity of current methods. The limits of detection and quantification were 0.05 and 0.2 mu g L-1, respectively, for histamine, cadaverine, spermine, and spermidine, 1.0 and 3.0 mu g L-1, respectively, for putrescine, 1.5 and 5.0 mu g L-1, respectively, for tyramine and tryptamine, and 2.0 and 5.0 mu g L-1, respectively, for 2-phenylethylamine. The recovery of biogenic amines from spiked water samples was between 97.3 and 108.6% at levels between 0.05 and 15 mu g L-1 (R > 0.999). The relative standard deviations were in the range of 0.10-0.29%. This method can achieve rapid and accurate determination of biogenic amines in surface water, and it meets the minimum residue measurement requirements.